Study on the crystallite and thermal properties of the nano-sized tricalcium phosphate by using XRD and DSC

Jan Ady; Sri Devi Ayu Ariska

doi:10.1063/5.0194075

Study on the crystallite and thermal properties of the nano-sized tricalcium phosphate by using XRD and DSC

Jan Ady, Sri Devi Ayu Ariska

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

Previously, the nano-sized tricalcium phosphate samples are prepared by the sol-gel method in this work. There are three samples of the nano-sized tricalcium phosphate resulted from its gel in the dry form, when temperature at 800 °C, 1000 °C, and 1200 °C are applied on the gel phases of the sample. After that, several parameters of the crystal characteristic have been confirmed by using the XRD to reveal the relevant parameters, such as the crystallite size, crystallite strain, crystallite dislocation, and crystallinity degree. Meanwhile, the thermal characteristics, such as the melting point, specific heat capacity, enthalpy of fusion, and crystallization enthalpy parameters, they are studied by using the DSC-TG.

Original language	English
Title of host publication	AIP Conference Proceedings
Editors	Tahta Amrillah, Gunawan Setia Prihandana, Rizki Putra Prastio, Prisma Megantoro, Indah Fahmiyah
Publisher	American Institute of Physics Inc.
Edition	1
ISBN (Electronic)	9780735448254
DOIs	https://doi.org/10.1063/5.0194075
Publication status	Published - 29 Jan 2024
Event	2nd International Conference on Advanced Technology and Multidiscipline: Supporting Sustainable Development Goals Through Innovation on Advanced Technology and Multidisciplinary Research, ICATAM 2022 - Virtual, Online, Indonesia Duration: 12 Oct 2022 → 13 Oct 2022

Publication series

Name	AIP Conference Proceedings
Number	1
Volume	3047
ISSN (Print)	0094-243X
ISSN (Electronic)	1551-7616

Conference

Conference	2nd International Conference on Advanced Technology and Multidiscipline: Supporting Sustainable Development Goals Through Innovation on Advanced Technology and Multidisciplinary Research, ICATAM 2022
Country/Territory	Indonesia
City	Virtual, Online
Period	12/10/22 → 13/10/22

Keywords

nano-sized
sol-gel
temperature
thermal
tricalcium phosphate

Access to Document

10.1063/5.0194075

Cite this

Ady, J., & Ariska, S. D. A. (2024). Study on the crystallite and thermal properties of the nano-sized tricalcium phosphate by using XRD and DSC. In T. Amrillah, G. S. Prihandana, R. P. Prastio, P. Megantoro, & I. Fahmiyah (Eds.), AIP Conference Proceedings (1 ed.). Article 050009 (AIP Conference Proceedings; Vol. 3047, No. 1). American Institute of Physics Inc.. https://doi.org/10.1063/5.0194075

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title = "Study on the crystallite and thermal properties of the nano-sized tricalcium phosphate by using XRD and DSC",

abstract = "Previously, the nano-sized tricalcium phosphate samples are prepared by the sol-gel method in this work. There are three samples of the nano-sized tricalcium phosphate resulted from its gel in the dry form, when temperature at 800 °C, 1000 °C, and 1200 °C are applied on the gel phases of the sample. After that, several parameters of the crystal characteristic have been confirmed by using the XRD to reveal the relevant parameters, such as the crystallite size, crystallite strain, crystallite dislocation, and crystallinity degree. Meanwhile, the thermal characteristics, such as the melting point, specific heat capacity, enthalpy of fusion, and crystallization enthalpy parameters, they are studied by using the DSC-TG.",

keywords = "nano-sized, sol-gel, temperature, thermal, tricalcium phosphate",

author = "Jan Ady and Ariska, {Sri Devi Ayu}",

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Ady, J & Ariska, SDA 2024, Study on the crystallite and thermal properties of the nano-sized tricalcium phosphate by using XRD and DSC. in T Amrillah, GS Prihandana, RP Prastio, P Megantoro & I Fahmiyah (eds), AIP Conference Proceedings. 1 edn, 050009, AIP Conference Proceedings, no. 1, vol. 3047, American Institute of Physics Inc., 2nd International Conference on Advanced Technology and Multidiscipline: Supporting Sustainable Development Goals Through Innovation on Advanced Technology and Multidisciplinary Research, ICATAM 2022, Virtual, Online, Indonesia, 12/10/22. https://doi.org/10.1063/5.0194075

Study on the crystallite and thermal properties of the nano-sized tricalcium phosphate by using XRD and DSC. / Ady, Jan; Ariska, Sri Devi Ayu.
AIP Conference Proceedings. ed. / Tahta Amrillah; Gunawan Setia Prihandana; Rizki Putra Prastio; Prisma Megantoro; Indah Fahmiyah. 1. ed. American Institute of Physics Inc., 2024. 050009 (AIP Conference Proceedings; Vol. 3047, No. 1).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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AU - Ariska, Sri Devi Ayu

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N2 - Previously, the nano-sized tricalcium phosphate samples are prepared by the sol-gel method in this work. There are three samples of the nano-sized tricalcium phosphate resulted from its gel in the dry form, when temperature at 800 °C, 1000 °C, and 1200 °C are applied on the gel phases of the sample. After that, several parameters of the crystal characteristic have been confirmed by using the XRD to reveal the relevant parameters, such as the crystallite size, crystallite strain, crystallite dislocation, and crystallinity degree. Meanwhile, the thermal characteristics, such as the melting point, specific heat capacity, enthalpy of fusion, and crystallization enthalpy parameters, they are studied by using the DSC-TG.

AB - Previously, the nano-sized tricalcium phosphate samples are prepared by the sol-gel method in this work. There are three samples of the nano-sized tricalcium phosphate resulted from its gel in the dry form, when temperature at 800 °C, 1000 °C, and 1200 °C are applied on the gel phases of the sample. After that, several parameters of the crystal characteristic have been confirmed by using the XRD to reveal the relevant parameters, such as the crystallite size, crystallite strain, crystallite dislocation, and crystallinity degree. Meanwhile, the thermal characteristics, such as the melting point, specific heat capacity, enthalpy of fusion, and crystallization enthalpy parameters, they are studied by using the DSC-TG.

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Study on the crystallite and thermal properties of the nano-sized tricalcium phosphate by using XRD and DSC

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Keywords

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