Preparation and Characterization ofAmorphous Silica Nano (SIO2) Based on Lumajang Sand Using Precipitation Method for Biomaterial Composite Applications

Dyah Hikmawati; Djony Izak Rudyardjo; Jan Ady; Erica Medina Ramadhaningtyas

doi:10.1063/5.0110262

Preparation and Characterization ofAmorphous Silica Nano (SIO₂) Based on Lumajang Sand Using Precipitation Method for Biomaterial Composite Applications

Siswanto, Dyah Hikmawati, Djony Izak Rudyardjo, Jan Ady, Erica Medina Ramadhaningtyas

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

1 Citation (Scopus)

Abstract

Research has been carried out on the synthesis of amorphous silica (SO2) made from Lumajang sand using the precipitation method. The use of this method is based on its simplicity and can produce large quantities. To increase the synthesis efficiency, nano sand was used, which was processed using high energy milling (HEM) for 15 hours and sintering temperature variations of500°C, 600⁰C, 700⁰C, 800°C, and 900⁰C. The results showed that the leaching process using 2M HCl could reduce crystal peaks and ball milling for 15 hours using HEM produces a sand particle size of 103.8 nm. From the XRD test of five sintering temperatures, amorphous silica occurs at a temperature of700⁰C, while at other temperatures, crystalline silica peaks still appear. This is supported by the degradation test data, which showed that amorphous silica sintered at 700⁰C had the highest rate.

Original language	English
Title of host publication	8th International Conference and Workshop on Basic and Applied Science, ICOWOBAS 2021
Editors	Anjar Tri Wibowo, M. Fariz Fadillah Mardianto, Riries Rulaningtyas, Satya Candra Wibawa Sakti, Muhammad Fauzul Imron, Rico Ramadhan
Publisher	American Institute of Physics Inc.
ISBN (Electronic)	9780735442610
DOIs	https://doi.org/10.1063/5.0110262
Publication status	Published - 25 Jan 2022
Event	8th International Conference and Workshop on Basic and Applied Science, ICOWOBAS 2021 - Surabaya, Indonesia Duration: 25 Aug 2021 → 26 Aug 2021

Publication series

Name	AIP Conference Proceedings
Volume	2554
ISSN (Print)	0094-243X
ISSN (Electronic)	1551-7616

Conference

Conference	8th International Conference and Workshop on Basic and Applied Science, ICOWOBAS 2021
Country/Territory	Indonesia
City	Surabaya
Period	25/08/21 → 26/08/21

Access to Document

10.1063/5.0110262

Cite this

Siswanto , Hikmawati, D., Rudyardjo, D. I., Ady, J., & Ramadhaningtyas, E. M. (2022). Preparation and Characterization ofAmorphous Silica Nano (SIO₂) Based on Lumajang Sand Using Precipitation Method for Biomaterial Composite Applications. In A. T. Wibowo, M. F. F. Mardianto, R. Rulaningtyas, S. C. W. Sakti, M. F. Imron, & R. Ramadhan (Eds.), 8th International Conference and Workshop on Basic and Applied Science, ICOWOBAS 2021 Article 060004 (AIP Conference Proceedings; Vol. 2554). American Institute of Physics Inc.. https://doi.org/10.1063/5.0110262

Siswanto, ; Hikmawati, Dyah ; Rudyardjo, Djony Izak et al. / Preparation and Characterization ofAmorphous Silica Nano (SIO₂) Based on Lumajang Sand Using Precipitation Method for Biomaterial Composite Applications. 8th International Conference and Workshop on Basic and Applied Science, ICOWOBAS 2021. editor / Anjar Tri Wibowo ; M. Fariz Fadillah Mardianto ; Riries Rulaningtyas ; Satya Candra Wibawa Sakti ; Muhammad Fauzul Imron ; Rico Ramadhan. American Institute of Physics Inc., 2022. (AIP Conference Proceedings).

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title = "Preparation and Characterization ofAmorphous Silica Nano (SIO2) Based on Lumajang Sand Using Precipitation Method for Biomaterial Composite Applications",

abstract = "Research has been carried out on the synthesis of amorphous silica (SO2) made from Lumajang sand using the precipitation method. The use of this method is based on its simplicity and can produce large quantities. To increase the synthesis efficiency, nano sand was used, which was processed using high energy milling (HEM) for 15 hours and sintering temperature variations of500°C, 6000C, 7000C, 800°C, and 9000C. The results showed that the leaching process using 2M HCl could reduce crystal peaks and ball milling for 15 hours using HEM produces a sand particle size of 103.8 nm. From the XRD test of five sintering temperatures, amorphous silica occurs at a temperature of7000C, while at other temperatures, crystalline silica peaks still appear. This is supported by the degradation test data, which showed that amorphous silica sintered at 7000C had the highest rate.",

author = "Siswanto and Dyah Hikmawati and Rudyardjo, {Djony Izak} and Jan Ady and Ramadhaningtyas, {Erica Medina}",

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Siswanto, , Hikmawati, D , Rudyardjo, DI , Ady, J & Ramadhaningtyas, EM 2022, Preparation and Characterization ofAmorphous Silica Nano (SIO₂) Based on Lumajang Sand Using Precipitation Method for Biomaterial Composite Applications. in AT Wibowo, MFF Mardianto, R Rulaningtyas, SCW Sakti, MF Imron & R Ramadhan (eds), 8th International Conference and Workshop on Basic and Applied Science, ICOWOBAS 2021., 060004, AIP Conference Proceedings, vol. 2554, American Institute of Physics Inc., 8th International Conference and Workshop on Basic and Applied Science, ICOWOBAS 2021, Surabaya, Indonesia, 25/08/21. https://doi.org/10.1063/5.0110262

Preparation and Characterization ofAmorphous Silica Nano (SIO₂) Based on Lumajang Sand Using Precipitation Method for Biomaterial Composite Applications. / Siswanto, ; Hikmawati, Dyah ; Rudyardjo, Djony Izak et al.
8th International Conference and Workshop on Basic and Applied Science, ICOWOBAS 2021. ed. / Anjar Tri Wibowo; M. Fariz Fadillah Mardianto; Riries Rulaningtyas; Satya Candra Wibawa Sakti; Muhammad Fauzul Imron; Rico Ramadhan. American Institute of Physics Inc., 2022. 060004 (AIP Conference Proceedings; Vol. 2554).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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T1 - Preparation and Characterization ofAmorphous Silica Nano (SIO2) Based on Lumajang Sand Using Precipitation Method for Biomaterial Composite Applications

AU - Siswanto,

AU - Hikmawati, Dyah

AU - Rudyardjo, Djony Izak

AU - Ady, Jan

AU - Ramadhaningtyas, Erica Medina

PY - 2022/1/25

Y1 - 2022/1/25

N2 - Research has been carried out on the synthesis of amorphous silica (SO2) made from Lumajang sand using the precipitation method. The use of this method is based on its simplicity and can produce large quantities. To increase the synthesis efficiency, nano sand was used, which was processed using high energy milling (HEM) for 15 hours and sintering temperature variations of500°C, 6000C, 7000C, 800°C, and 9000C. The results showed that the leaching process using 2M HCl could reduce crystal peaks and ball milling for 15 hours using HEM produces a sand particle size of 103.8 nm. From the XRD test of five sintering temperatures, amorphous silica occurs at a temperature of7000C, while at other temperatures, crystalline silica peaks still appear. This is supported by the degradation test data, which showed that amorphous silica sintered at 7000C had the highest rate.

AB - Research has been carried out on the synthesis of amorphous silica (SO2) made from Lumajang sand using the precipitation method. The use of this method is based on its simplicity and can produce large quantities. To increase the synthesis efficiency, nano sand was used, which was processed using high energy milling (HEM) for 15 hours and sintering temperature variations of500°C, 6000C, 7000C, 800°C, and 9000C. The results showed that the leaching process using 2M HCl could reduce crystal peaks and ball milling for 15 hours using HEM produces a sand particle size of 103.8 nm. From the XRD test of five sintering temperatures, amorphous silica occurs at a temperature of7000C, while at other temperatures, crystalline silica peaks still appear. This is supported by the degradation test data, which showed that amorphous silica sintered at 7000C had the highest rate.

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BT - 8th International Conference and Workshop on Basic and Applied Science, ICOWOBAS 2021

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A2 - Mardianto, M. Fariz Fadillah

A2 - Rulaningtyas, Riries

A2 - Sakti, Satya Candra Wibawa

A2 - Imron, Muhammad Fauzul

A2 - Ramadhan, Rico

PB - American Institute of Physics Inc.

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Y2 - 25 August 2021 through 26 August 2021

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Siswanto , Hikmawati D , Rudyardjo DI , Ady J, Ramadhaningtyas EM. Preparation and Characterization ofAmorphous Silica Nano (SIO₂) Based on Lumajang Sand Using Precipitation Method for Biomaterial Composite Applications. In Wibowo AT, Mardianto MFF, Rulaningtyas R, Sakti SCW, Imron MF, Ramadhan R, editors, 8th International Conference and Workshop on Basic and Applied Science, ICOWOBAS 2021. American Institute of Physics Inc. 2022. 060004. (AIP Conference Proceedings). doi: 10.1063/5.0110262