4-({4-[(2E)-3-(2,5-dimethoxyphenyl)Prop-2-Enoyl]phenyl}amino)-4-Oxobutanoic acid

Hery Suwito; Kautsar Ul Haq; Nia Nur Dinia Rahmah; Alfinda Novi Kristanti; Ni Nyoman Tri Puspaningsih

doi:10.3390/M938

4-({4-[(2E)-3-(2,5-dimethoxyphenyl)Prop-2-Enoyl]phenyl}amino)-4-Oxobutanoic acid

Hery Suwito, Kautsar Ul Haq, Nia Nur Dinia Rahmah, Alfinda Novi Kristanti, Ni Nyoman Tri Puspaningsih

Research output: Contribution to journal › Comment/debate

4 Citations (Scopus)

Abstract

A dimethoxy amide chalcone has been synthesized in a two-step reaction. First, an amine chalcone was synthesized by the reaction of 4′-aminoacetophenone and 2,5-dimethoxybenzaldehyde using 40% NaOH solution as a catalyst in ethanol, and then followed by amidation through the reaction of the formed chalcone and succinic anhydride. The structure of the target compound was established by FTIR, HR-MS,¹H-and¹³C-NMR, and 2D-NMR spectral analysis.

Original language	English
Article number	M938
Journal	MolBank
Volume	2017
Issue number	2
DOIs	https://doi.org/10.3390/M938
Publication status	Published - Jun 2017

Keywords

Amide chalcones
Amino chalcones
Succinic anhydride

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@article{5ce6b35b5c7d44168ec949443cc441d8,

title = "4-({4-[(2E)-3-(2,5-dimethoxyphenyl)Prop-2-Enoyl]phenyl}amino)-4-Oxobutanoic acid",

abstract = "A dimethoxy amide chalcone has been synthesized in a two-step reaction. First, an amine chalcone was synthesized by the reaction of 4′-aminoacetophenone and 2,5-dimethoxybenzaldehyde using 40% NaOH solution as a catalyst in ethanol, and then followed by amidation through the reaction of the formed chalcone and succinic anhydride. The structure of the target compound was established by FTIR, HR-MS,1H-and13C-NMR, and 2D-NMR spectral analysis.",

keywords = "Amide chalcones, Amino chalcones, Succinic anhydride",

author = "Hery Suwito and Haq, {Kautsar Ul} and Rahmah, {Nia Nur Dinia} and Kristanti, {Alfinda Novi} and Puspaningsih, {Ni Nyoman Tri}",

note = "Publisher Copyright: {\textcopyright} 2017 by the authors. Licensee MDPI, Basel, Switzerland.",

year = "2017",

month = jun,

doi = "10.3390/M938",

language = "English",

volume = "2017",

journal = "MolBank",

issn = "1422-8599",

publisher = "Multidisciplinary Digital Publishing Institute (MDPI)",

number = "2",

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TY - JOUR

T1 - 4-({4-[(2E)-3-(2,5-dimethoxyphenyl)Prop-2-Enoyl]phenyl}amino)-4-Oxobutanoic acid

AU - Suwito, Hery

AU - Haq, Kautsar Ul

AU - Rahmah, Nia Nur Dinia

AU - Kristanti, Alfinda Novi

AU - Puspaningsih, Ni Nyoman Tri

PY - 2017/6

Y1 - 2017/6

N2 - A dimethoxy amide chalcone has been synthesized in a two-step reaction. First, an amine chalcone was synthesized by the reaction of 4′-aminoacetophenone and 2,5-dimethoxybenzaldehyde using 40% NaOH solution as a catalyst in ethanol, and then followed by amidation through the reaction of the formed chalcone and succinic anhydride. The structure of the target compound was established by FTIR, HR-MS,1H-and13C-NMR, and 2D-NMR spectral analysis.

AB - A dimethoxy amide chalcone has been synthesized in a two-step reaction. First, an amine chalcone was synthesized by the reaction of 4′-aminoacetophenone and 2,5-dimethoxybenzaldehyde using 40% NaOH solution as a catalyst in ethanol, and then followed by amidation through the reaction of the formed chalcone and succinic anhydride. The structure of the target compound was established by FTIR, HR-MS,1H-and13C-NMR, and 2D-NMR spectral analysis.

KW - Amide chalcones

KW - Amino chalcones

KW - Succinic anhydride

UR - http://www.scopus.com/inward/record.url?scp=85018963760&partnerID=8YFLogxK

U2 - 10.3390/M938

DO - 10.3390/M938

M3 - Comment/debate

AN - SCOPUS:85018963760

SN - 1422-8599

VL - 2017

JO - MolBank

JF - MolBank

IS - 2

M1 - M938

ER -

4-({4-[(2E)-3-(2,5-dimethoxyphenyl)Prop-2-Enoyl]phenyl}amino)-4-Oxobutanoic acid

Abstract

Keywords

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